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ASTM D 5453 REV B Document Information:
Title
Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM International
Publication Date:
Jul 1, 2008
Scope:
This test method covers the determination of total sulfur in
liquid hydrocarbons, boiling in the range from approximately 25 to
400°C, with viscosities between approximately 0.2 and 20 cSt
(mm2/S) at room temperature.
Three separate interlaboratory studies (ILS) on precision, and
three other investigations that resulted in an ASTM research
report, have determined that this test method is applicable to
naphthas, distillates, engine oil, ethanol, Fatty Acid Methyl Ester
(FAME), and engine fuel such as gasoline, oxygen enriched gasoline
(ethanol blends, E-85, M-85, RFG), diesel, biodiesel,
diesel/biodiesel blends, and jet fuel. Samples containing 1.0 to
8000 mg/kg total sulfur can be analyzed (Note 1).
NOTE 1—Estimates of the pooled limit of quantification (PLOQ)
for the precision studies were calculated. Values ranged between
less than 1.0 and less than 5.0 mg/kg (see Section 8 and 15.1).
This test method is applicable for total sulfur determination in
liquid hydrocarbons containing less than 0.35 % (m/m)
halogen(s).
The values stated in SI units are to be regarded as standard. No
other units of measurement are included in this standard.
This standard does not purport to address all of the safety
concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and
health practices and determine the applicability of regulatory
limitations prior to use. For warning statements, see 3.1,
6.3, 6.4, Section 7, and 8.1.
*A Summary of Changes section appears at the end of this
standard.
Keywords:
- analysis
- biodiesel
- biodiesel-fuel blends
- E-85
- ethanol
- ethanol-fuel blends
- diesel
- fluorescence
- gasoline
- jet fuel
- kerosine
- M-85
- RFG
- sulfur
- ultraviolet
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